How To Measure Glass Transition Temperature. In DSC the difference in heat flow to a sample and to a reference is monitored against time or temperature while the. While there are several options for the test type flexural strength or shear strength testing are the standards. Crystalline polymers exhibit a Tm melt temperature and typically a Tg since there is usually an amorphous portion as well semi-crystalline. It is necessary to rely in a reasonable personal judgement.
It can be determined according to various standard methods eg. As the temperature increases an amorphous solid will become less viscous. Most notably these include. As the temperature at half the step height or as the point of intersection of the bisector of the angle between the tangents with the measurement. Since performing a series of tests at increasing temperatures is time. No formal phase change occurs.
The specific Tg value often depends upon the method and parameters employed so care must be.
No formal phase change occurs. Most notably these include. Crystalline polymers exhibit a Tm melt temperature and typically a Tg since there is usually an amorphous portion as well semi-crystalline. It can be determined according to various standard methods eg. Glass Transition is a method to characterize a property of a polymeric material. The specific Tg value often depends upon the method and parameters employed so care must be.